Preparation of high surface area TiO (anatase) by thermal hydrolysis 2 of titanyl sulphate solution

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Preparation of high surface area TiO (anatase) by thermal hydrolysis 2 of titanyl sulphate solution

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dc.contributor.author Mohammed Yusuff,K K
dc.contributor.author Ahmed Yasir,Vakayil
dc.contributor.author Mohandas,P N
dc.date.accessioned 2010-04-24T06:24:15Z
dc.date.available 2010-04-24T06:24:15Z
dc.date.issued 2001-08-12
dc.identifier.citation Applied Chemistry,Cochin University of Science and Technology en_US
dc.identifier.other PII: S1466-6049(01)00171-4
dc.identifier.other International Journal of Inorganic Materials 3 (2001) 593 –596
dc.identifier.uri http://dyuthi.cusat.ac.in/purl/1647
dc.description.abstract Highly crystalline, ultra fine TiO (anatase) having high surface area has been prepared by thermal hydrolysis of titanyl sulphate 2 solution and characterized using B.E.T surface area measurements, XRD and chemical analysis. The dependence of surface area on concentration of staffing solution, temperature of hydrolysis, duration of boiling and calcination temperature were also studied. As the boiling temperature, duration of boiling and calcination temperature increased, the surface area of TiO formed decreased significantly. 2 On increasing calcination temperature, the crystallite size of TiO also increased and gradually the phase transformation to rutile took 2 place. The onset and completion temperatures of rutilation were 700 and 10008C, respectively en_US
dc.language.iso en en_US
dc.publisher Elsevier, International Journal of Inorganic Materials en_US
dc.subject Thermal hydrolysis en_US
dc.subject Titanyl sulphate en_US
dc.subject Crystalline en_US
dc.subject Anatase en_US
dc.subject Surface area and rutilation en_US
dc.title Preparation of high surface area TiO (anatase) by thermal hydrolysis 2 of titanyl sulphate solution en_US
dc.type Working Paper en_US


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